000			021510000a22005770004500
911			_aXL1991005624
901			_aQ04
903			_aE
903			_aV
904			_aBCO
905			_aC
906			_a19910101
908			_aJ
909			_aAS
912			_aEn
912			_aEn
914			_aCACAO
914			_aEXTRA
914			_aBCO1
082	0	4	_a633.746 _bS855
100	1		_9121809 _aStijve, T.
100	1		_962789 _aDiserens, H.
260			_cJun 1987
041	0		_aEn
500			_a2 tab. 10 ref. Sum. (De, En)
520			_aA method is presented for the isolation of polycyclic aromatic hydrocarbons (PAHs) from large test portions of fats and oils: 30 g of lipid material are adsorbed on synthetic calcium silicate (Calflo E) and extracted with a mixture of acetonitrile-acetone 9:1. The evaporated extract containing only small amounts of co-extracted fat is subjected to one of the current methods for PAH analysis. The technique is also applicable to difficult substrates as lecithin, spice oleoresins and essential oils. Recoveries for several PAHs including benzo(a)pyrene ranged from 72-87 percent.
650	1	4	_9153864 _aMANTECA DE CACAO
650	1	4	_9150294 _aHIDROCARBUROS AROMATICOS
650	1	4	_9137749 _aBENZOPIRENOS
650	1	4	_9153173 _aLIPIDOS
650	1	4	_9164583 _aSILICATES
650	1	4	_9147509 _aEXTRACCION
650	1	4	_9163877 _aSAPONIFICACION
691			_9311335 _aCOCOA BUTTER
691			_9306476 _aAROMATIC HYDROCARBONS
691			_9307698 _aBENZOPYRENE
691			_9325297 _aLIPIDS 04 CERAMIDES
691			_9318589 _aEXTRACTION
691			_9337435 _aSAPONIFICATION
692			_aBEURRE DE CACAO
692			_aHYDROCARBURE AROMATIQUE
692			_aBENZOPYRENE
692			_aLIPIDE
692			_aEXTRACTION
692			_aSAPONIFICATION
773	0		_tDeutsche Lebensmittel-Rundschau (Alemania) _dJun 1987 _gv. 83(6) p. 183-185
040			_aCR-TuBCO _cCR-TuBCO _bEs
245	1	0	_aThe use of calflo E solid support for extraction of benzo(a)pyrene and other polycyclic aromatic hydrocarbons from large quantities of fats and oils
942			_cANA
003			CR-TuBCO
999			_c71566 _d71566